Analytical Sciences


Cover image of volume 37, number 11

Volume 37, Number 11 (2021)

Cover illustration of this month"Relationship between Width and Height of π* Peak in C K-XANES of Graphitic Carbons" by Yasuji MURAMATSU, Kentaro MURAYAMA, Toru OKADA, and Tsuyoshi OOE (p.1617). See larger image


Highlights − Volume 37, Number 11 (2021)

Quantitative NMR in Analytical Chemistry
Hideshi MAKI
Keywords: qNMR, quantitative NMR
Analytical Sciences, 2021, 37(11), 1485.
DOI: 10.2116/analsci.highlights2111
figure


Hot Articles − Volume 37, Number 11 (2021)

hot article mark
Quantification of Enterohemorrhagic Escherichia coli via Optical Nanoantenna and Temperature-responsive Artificial Antibodies
So TANABE,* Satohiro ITAGAKI,* Shuyi SUN,* Kyohei MATSUI,* Takamasa KINOSHITA,* Shigeki NISHII,* Yojiro YAMAMOTO,*,** Yasuhiro SADANAGA,* and Hiroshi SHIIGI
Keywords: Temperature-responsive artificial antibodies, light-scattering, molecular imprinting polymer, dark-field microscope, enterohemorrhagic Escherichia coli
Analytical Sciences, 2021, 37(11), 1597.
DOI: 10.2116/analsci.21P135


Table of Contents − Volume 37, Number 11 (2021)

Highlights

Quantitative NMR in Analytical Chemistry
Hideshi MAKI
Keywords: qNMR, quantitative NMR
Analytical Sciences, 2021, 37(11), 1485.
DOI: 10.2116/analsci.highlights2111
figure

Rapid Communications

Highly Sensitive Alkaline Phosphatase Biosensor Based on Internal Filtration Effect between G-Quadruplex/N-methylmesoporphyrin IX and p-Nitrophenol
Liyuan MA,* Yao XIAO,* Huajuan FANG,* Hualin YANG,*,** and Yu ZHOU
Keywords: Alkaline phosphatase, G-quadruplex, p-nitrophenol, inner filter effect, biosensor
Analytical Sciences, 2021, 37(11), 1487.
DOI: 10.2116/analsci.21C010
figure

TLC-based MS Imaging Analysis of Glycosphingolipids and Glycerin Fatty Acid Esters after 1,2-Dichloroethane Washing
Shoko MATSUSHITA, Takuma HASEGAWA, Marina HIRAOKA, Aki HAYASHI, and Yusuke SUZUKI
Keywords: 1,2-Dichloroethane, glycosphingolipid, glycerin fatty acid ester, mass spectrometry imaging, thin-layer chromatography
Analytical Sciences, 2021, 37(11), 1491.
DOI: 10.2116/analsci.21C009
figure

Original Papers

Pristine Graphic Carbon Nitride Quantum Dots for the Visualized Detection of Latent Fingerprints
Haidong LI,* Chenyao ZHANG,** Jun WANG,* Hui CHONG,* Tian ZHANG,* and Chengyin WANG
Keywords: Graphic carbon nitride quantum dots, low temperature solid-phase reaction, latent fingerprint, visualized detection
Analytical Sciences, 2021, 37(11), 1497.
DOI: 10.2116/analsci.20P336
figure

Visualization of the Orientation of Amphipathic Peptides at the Air–Water Interface by X-Ray Reflectometry
Mari OKUNO,* Makoto ITAGAKI,** Taka-aki ISHIBASHI,** and Yohko F. YANO
Keywords: X-ray reflectometry, LKα14 peptide, air–water interface, electron density profiles, monolayer
Analytical Sciences, 2021, 37(11), 1505.
DOI: 10.2116/analsci.21P068
figure

Nylon Monofilament Mold Three-dimensional Microfluidic Chips for Size-exclusion Microchip Electrophoresis: Application to Specific Online Preconcentration of Proteins
Sachio YAMAMOTO,* Kazuhito MAETANI,* Gai TATSUMI,* Fuka OKADA,* Mitsuhiro KINOSHITA,* and Shigeo SUZUKI
Keywords: Nylon monofilaments mold, dialysis membrane, online concentration, online purification, microchip electrophoresis
Analytical Sciences, 2021, 37(11), 1511.
DOI: 10.2116/analsci.21P080
figure

Optimization of Procedure for Determining Dissolved Oxygen in Surface Water and Seawater Exploiting the UV-vis Absorption of Mn(III) Species
Tu DANG,* Yasuaki MAEDA,** Yusuke FUJII,* and Norimichi TAKENAKA
Keywords: Dissolved oxygen, photometric method, the Winkler method, surface water, seawater
Analytical Sciences, 2021, 37(11), 1517.
DOI: 10.2116/analsci.21P079
figure

A Sensitive Signal-on Supersandwich DNA Biosensor Based on the Enhancement of Poly(aniline-luminol) Nanowires Electrochemiluminescence by Ferrocene
Zhifang DING, Yue LI, Ying BAO, Kexin HAN, Iparguli TUREPU, and Guixin LI
Keywords: Electrochemiluminescence, poly(aniline-luminol) nanowires, ferrocene, supersandwich, DNA biosensor
Analytical Sciences, 2021, 37(11), 1525.
DOI: 10.2116/analsci.21P027
figure

Development of a Polystyrene Reference Material for Raman Spectrometer (NMIJ RM 8158-a)
Nobuyasu ITOH and Nobuyasu HANARI
Keywords: Reference material, polystyrene, Raman shift, HeNe laser, emission lines, uncertainty
Analytical Sciences, 2021, 37(11), 1533.
DOI: 10.2116/analsci.21P054
figure

A Fast Dual-responsive OFF-ON Fluorescent Probe for Cysteine and Glutathione without Interference from Homocysteine
Qingjie FU,* Ruxin LIU,* Xiaoqian CUI,** Yuqi ZHAO,* Hui CHI,* Yongzhuang LU,* Qiang FEI,* Guodong FENG,* Hongyan SHAN,* and Yanfu HUAN
Keywords: Organic small molecule, fluorescent off-on probe, biothiols discrimination, dual responsive, interference elimination, fast sensing
Analytical Sciences, 2021, 37(11), 1541.
DOI: 10.2116/analsci.21P088
figure

Magnetic Solid-Phase Extraction Based on Amino-functionalized Magnetic Starch for Analysis of Organochlorine Pesticides
Dana Ayu MUSTOFA, Jirasak GAMONCHUANG, and Rodjana BURAKHAM
Keywords: Solid phase extraction, magnetic material, diaminobenzoic acid, aminopropyltriethoxysilane, organochlorine, gas chromatography
Analytical Sciences, 2021, 37(11), 1547.
DOI: 10.2116/analsci.21P034
figure

Simplification of Moment Analysis Procedure for Kinetic Study of Chromatographic Behavior of Core-shell Particles
Kanji MIYABE
Keywords: Moment theory, simple moment analysis, core-shell column, spherical core-shell particle, mass transfer kinetics, intra-stationary phase diffusion
Analytical Sciences, 2021, 37(11), 1553.
DOI: 10.2116/analsci.21P094
figure

Improvement of Extractive Alkylation Gas Chromatography of Short-chain Carboxylic Acids in Aqueous Solution
Shigemi UEDA,* Noriyuki TAKEMOTO,** Risa ONODERA,** Shinji TSUNOI,*** and Ikuya SHIBATA
Keywords: Extractive alkylation, gas chromatography, pentafluorobenzylation, short-chain carboxylic acids, formic acid, acetic acid, removal of tetrahexylammonium bromide, perchloric acid
Analytical Sciences, 2021, 37(11), 1559.
DOI: 10.2116/analsci.21P073
figure

Chemical State Analysis of Heavy Metals and Radioactive Cesium in Municipal Solid Waste Incineration Fly Ash Contaminated with Radioactive Cesium Released by the FDNPP Accident
Yuya KOIKE,* Kengo FUJII,** Rintaro SAITO,** Narihito OGAWA,* and Atsushi OHBUCHI
Keywords: Municipal solid waste incineration fly ash, chemical states, sequential extraction test, heavy metals, radioactive Cs
Analytical Sciences, 2021, 37(11), 1565.
DOI: 10.2116/analsci.21P022
figure

Comparative Evaluation of Natural Killer Cell-mediated Cell Killing Assay Based on the Leakage of an Endogenous Enzyme or a Pre-loaded Fluorophore
Kenta TANITO,*1 Yunosuke OSHIRO,*1 Hiroshi TAGAWA,*1 Akihiro KISHIMURA,*1,*2,*3 Takeshi MORI,*1,*2 and Yoshiki KATAYAMA
Keywords: Antibody dependent cellular cytotoxicity, lactate dehydrogenase, calcein-AM, probenecid
Analytical Sciences, 2021, 37(11), 1571.
DOI: 10.2116/analsci.21P117
figure

Quantification of Cathinone Analogues without Reference Standard Using 1H Quantitative NMR
Yuxin ZHAO,*1,*2 Bo WU,*1,*3 Zhendong HUA,*2,*4 Peng XU,*2,*4 Hui XU,*1,*2 Wenbin SHEN,*5 Bin DI,*1,*2 Youmei WANG,*2,*4 and Mengxiang SU
Keywords: Quantitative nuclear magnetic resonance, assay, synthetic cathinones, structure identification, quantitation
Analytical Sciences, 2021, 37(11), 1577.
DOI: 10.2116/analsci.21P048
figure

A Simple Colorimetric Analytical Assay for the Determination of Tetracyclines Based on In-situ Generation of Gold Nanoparticles Coupling with a Gold Staining Technique
Ningning YUE, Dongmei LI, and Aiping FAN
Keywords: Colorimetric method, tetracyclines, gold nanoparticles, gold staining, milk
Analytical Sciences, 2021, 37(11), 1583.
DOI: 10.2116/analsci.21P115
figure

Molten-salt-composite of Pyrite and Silver Nanoparticle as Electrocatalyst for Hydrogen Peroxide Sensing
Jifan ZHAO,* Yue WANG,* Ting WANG,** Yasushi HASEBE,*** and Zhiqiang ZHANG
Keywords: Pyrite, silver nanoparticles, molten salt method, hydrogen peroxide, electrochemical sensor
Analytical Sciences, 2021, 37(11), 1589.
DOI: 10.2116/analsci.21P119
figure

hot article mark
Quantification of Enterohemorrhagic Escherichia coli via Optical Nanoantenna and Temperature-responsive Artificial Antibodies
So TANABE,* Satohiro ITAGAKI,* Shuyi SUN,* Kyohei MATSUI,* Takamasa KINOSHITA,* Shigeki NISHII,* Yojiro YAMAMOTO,*,** Yasuhiro SADANAGA,* and Hiroshi SHIIGI
Keywords: Temperature-responsive artificial antibodies, light-scattering, molecular imprinting polymer, dark-field microscope, enterohemorrhagic Escherichia coli
Analytical Sciences, 2021, 37(11), 1597.
DOI: 10.2116/analsci.21P135
figure

Separation of Light and Middle Lanthanides Using Multistage Extraction with Diglycolamide Extractant
Takafumi MATSUTANI,*,** Yuji SASAKI,* and Shoichi KATSUTA
Keywords: Lanthanide separation, solvent extraction, multistage extraction, DGA extractant
Analytical Sciences, 2021, 37(11), 1603.
DOI: 10.2116/analsci.21P120
figure

Stable Formation of Aqueous/Organic Parallel Two-phase Flow in Nanochannels with Partial Surface Modification
Hiroki SANO,*1 Yutaka KAZOE,*1,*2 and Takehiko KITAMORI
Keywords: Nanofluidics, nanochannel, multiphase flow, bonding, surface modification, focused ion beam, femtoliter
Analytical Sciences, 2021, 37(11), 1611.
DOI: 10.2116/analsci.21P138
figure

Relationship between Width and Height of π* Peak in C K-XANES of Graphitic Carbons
Yasuji MURAMATSU, Kentaro MURAYAMA, Toru OKADA, and Tsuyoshi OOE
Keywords: Graphitic carbon, edge carbon, C K-XANES, π* peak, local structure
Analytical Sciences, 2021, 37(11), 1617.
DOI: 10.2116/analsci.21P139
figure

Notes

Applicability of Superheated Water Extraction for the Quantification of Pesticide Residues in Leafy Vegetables
Takashi YARITA, Atsuhiko HASEGAWA, and Hiroko TADA
Keywords: Superheated water extraction, residual pesticides, organophosphorus pesticides, fenitrothion, gas chromatography–mass spectrometry, octanol–water partition coefficient
Analytical Sciences, 2021, 37(11), 1625.
DOI: 10.2116/analsci.21N003
figure

Characteristics of Electrospray-Ionization Detection of Synthetic Di- to Penta-Oligopeptides by Amine Derivatizations
Weilin SHEN, Kiyomi ONO, Mitsuru TANAKA, and Toshiro MATSUI
Keywords: Oligopeptide, ESI-MS, chemical derivatization, molecular surface area
Analytical Sciences, 2021, 37(11), 1629.
DOI: 10.2116/analsci.21N016
figure

How Feasible is Direct Determination of Rare Earth Elements in Seawater by ICP-MS?
Olga V. KUZNETSOVA, Nikita V. DUSHENKO, and Andrei R. TIMERBAEV
Keywords: Rare earth elements, analysis of seawater, ICP-MS, dilution, validation
Analytical Sciences, 2021, 37(11), 1633.
DOI: 10.2116/analsci.21N012
figure

Size Analysis of Small Metal Nanoparticles Using Single Particle ICP Mass Spectrometry
Shuji YAMASHITA, Masaki NAKAZATO, and Takafumi HIRATA
Keywords: Nanoparticle, ICP-MS, desolvating system, deconvolution method, size detection limit
Analytical Sciences, 2021, 37(11), 1637.
DOI: 10.2116/analsci.21N014
figure

Adsorption Behavior of Pu(IV), Am(III), Cm(III), and U(VI) on Desferrioxamine B-immobilized Micropolymer and Its Applications in the Separation of Pu(IV)
Jo AOKI,*1 Chisa OONUMA,*2 Ralf SUDOWE,*3 and Yoshitaka TAKAGAI
Keywords: Desferrioxamine B-immobilized micropolymeric resin, plutonium, americium, curium, uranium, adsorption, separation
Analytical Sciences, 2021, 37(11), 1641.
DOI: 10.2116/analsci.21N028
figure

Advancements in Instrumentation

Building a Scanning Probe Microscope Using Open Source Control Software and Systems
Shinya KISHIOKA
Keywords: SPM, STM, FM-AFM, tuning fork, open-source control software, GXSM
Analytical Sciences, 2021, 37(11), 1645.
DOI: 10.2116/analsci.21A004
figure

Announcements

Analytical Sciences, 2021, 37(11), 1651.
DOI: 10.2116/analsci.announce2111